Microstructure Evolution Characteristics of Industrial Electrolytic Nickel Deposits

	Microstructure Evolution Characteristics of Industrial Electrolytic Nickel Deposits
	Xu, Yangtao1,2,3 ; Wang, Chao 1; Liu, Zhijian 1; Lu, Jianbo 2; Su, Yujuan 2
	2022-04-01
发表期刊	Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering
ISSN	1002-185X
卷号	51 期号:4 页码:1462-1469
摘要	This work studied the characteristics of the microstructure of industrial electrolytic nickel deposits changing with deposition time. Using XRD, SEM, EBSD and other analysis methods, the preferred orientation, microstructure and characteristic grain boundary distribution of electrolytic nickel plate with the deposition time were studied. The results show that the crystals on the surface of the electrodeposited nickel plate mainly grow in the direction perpendicular to the (200) plane, the cross-section shows the (111) and (200) double preferred orientations, and the crystal growth method is lateral growth. The surface and the cross-section show different microstructures. The surface morphology changes from a pyramid shape to a cell shape and the growth mechanism changes from spiral dislocation-driven growth to atomic aggregation and accumulation. The cross-sectional morphology of the nickel plate is always a lamellar structure at each stage. The cross-section of the deposited layer is mainly high-angle grain boundaries and a large number of Σ3 twin grain boundaries. In the stable growth process, the proportion of large-angle grain boundaries gradually decreases as the deposition progresses, nevertheless the relative frequency of Σ3 grain boundaries gradually increases, but they will all be affected by changes in the environment of the electrolytic cell. In the cross-section along the growth direction, the electrolytic nickel plate mainly shows the fiber texture of direction, and a large number of Σ3 twin boundaries affect the orientation of the deposited layer. By increasing the ratio of Σ3 twin boundaries or selecting the electrolytic nickel corresponding to the higher frequency of Σ3 twin boundaries, electrolytic nickel with better strength and plasticity can be obtained. The evolution law of the electrolytic nickel deposition layer has been clarified, which means that the micro-control of the electrolytic nickel organization can be carried out in the later research or the guidance of industrial production, and the customized production of electrolytic nickel under industrial conditions can be realized. © 2022, Science Press. All right reserved.
关键词	Crystal orientation Grain boundaries Industrial research Lamellar structures Morphology Nickel Plates (structural components) Surface morphology Textures Deposited layer Deposition time EBSD Electrolytics Evolution characteristics Grain-boundaries Industrial electrolytic nickel Microstructure evolutions Preferred orientations Twin boundaries
收录类别	EI
语种	中文
出版者	Science Press
EI入藏号	20222012120358
EI主题词	Deposition
EI分类号	408.2 Structural Members and Shapes ; 548.1 Nickel ; 801.4 Physical Chemistry ; 802.3 Chemical Operations ; 901.3 Engineering Research ; 912.1 Industrial Engineering ; 931.2 Physical Properties of Gases, Liquids and Solids ; 933.1.1 Crystal Lattice ; 951 Materials Science
文献类型	期刊论文
条目标识符	https://ir.lut.edu.cn/handle/2XXMBERH/158370
专题	省部共建有色金属先进加工与再利用国家重点实验室
作者单位	1.State Key Laboratory of Advanced Processing and Recycling of Non-Ferrous Metal, Lanzhou University of Technology, Lanzhou; 730050, China; 2.State Key Laboratory for Comprehensive Utilization of Nickel and Cobalt Resources, Jinchang; 737100, China; 3.Baiyin Novel Materials Research Institute, Lanzhou University of Technology, Baiyin; 730900, China
第一作者单位	兰州理工大学
第一作者的第一单位	兰州理工大学
推荐引用方式 GB/T 7714	Xu, Yangtao,Wang, Chao,Liu, Zhijian,et al. Microstructure Evolution Characteristics of Industrial Electrolytic Nickel Deposits[J]. Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering,2022,51(4):1462-1469.
APA	Xu, Yangtao,Wang, Chao,Liu, Zhijian,Lu, Jianbo,&Su, Yujuan.(2022).Microstructure Evolution Characteristics of Industrial Electrolytic Nickel Deposits.Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering,51(4),1462-1469.
MLA	Xu, Yangtao,et al."Microstructure Evolution Characteristics of Industrial Electrolytic Nickel Deposits".Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering 51.4(2022):1462-1469.