Institutional Repository of Coll Life & Sci Engn
A Mixed Micellar Liquid Chromatography with Direct Injection for Rapid Analysis of Eight Sulfonamides in Milk | |
Duan, Xiaoyun1,2; Liu, Xiaofeng2; Dong, Yue1; Duan, Tianjiao2; Zhang, Jing1; He, Shujuan1; Yang, Fatang1; Dong, Yuming1 | |
2020-05 | |
发表期刊 | Food Analytical Methods |
ISSN | 19369751 |
卷号 | 13期号:5页码:1148-1158 |
摘要 | In this work, an isocratic mixed micellar liquid chromatography method was first applied to the separation of eight sulfonamides in milk. Mixed anionic and nonionic surfactants were used as mobile phase additives. Because proteins in the milk can be dissolved by the micelles, the milk samples can be directly injected into the chromatographic system after being simply diluted 10 times with 0.1 M sodium dodecyl sulfate solution. Besides, three-phase equilibrium theory was firstly used to explain the retention mechanism of sulfonamides in the mixed micellar liquid chromatography. The optimized mobile phase was an aqueous solution (0.04 M sodium dodecyl sulfate and 0.01 M polyoxyethylene lauryl ether) containing 20 mM NaH2PO4 with 10% (v/v) of n-propanol at pH 3.0. The separation was performed on a Venusil XBP C18 column (250 × 4.6 mm, i.d., 5 μm). The proposed mixed micellar liquid chromatography method was validated in terms of linear ranges (20–2500 μg/L), limit of detections (1.9–8.0 μg/L), limit of quantitations (6.1–27 μg/L), recoveries (84–105%), intra- and inter-precisions (RSD © 2020, Springer Science+Business Media, LLC, part of Springer Nature. |
关键词 | Additives Amides Dairies Direct injection Liquids Micelles Nonionic surfactants Polyethylene oxides Separation Sodium dodecyl sulfate Sulfur compounds Chromatographic systems Limit of quantitations Micellar liquid chromatography Mobile phase additives Polyoxyethylene lauryl ethers Retention mechanism Sodium dodecyl sulfate solutions Three-phase equilibria |
DOI | 10.1007/s12161-020-01733-3 |
收录类别 | EI ; SCIE |
语种 | 英语 |
WOS研究方向 | Food Science & Technology |
WOS类目 | Food Science & Technology |
WOS记录号 | WOS:000517683100002 |
出版者 | Springer |
EI入藏号 | 20201108301121 |
EI主题词 | Liquid chromatography |
EI分类号 | 521 Fuel Combustion and Flame Research ; 801.3 Colloid Chemistry ; 802.3 Chemical Operations ; 803 Chemical Agents and Basic Industrial Chemicals ; 804.1 Organic Compounds ; 815.1.1 Organic Polymers ; 822.1 Food Products Plants and Equipment |
来源库 | WOS |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | https://ir.lut.edu.cn/handle/2XXMBERH/151039 |
专题 | 生命科学与工程学院 |
通讯作者 | Dong, Yue |
作者单位 | 1.Lanzhou Univ, Sch Pharm, Lanzhou, Peoples R China; 2.Lanzhou Univ Technol, Sch Life Sci & Engn, Lanzhou, Peoples R China |
第一作者单位 | 生命科学与工程学院 |
推荐引用方式 GB/T 7714 | Duan, Xiaoyun,Liu, Xiaofeng,Dong, Yue,et al. A Mixed Micellar Liquid Chromatography with Direct Injection for Rapid Analysis of Eight Sulfonamides in Milk[J]. Food Analytical Methods,2020,13(5):1148-1158. |
APA | Duan, Xiaoyun.,Liu, Xiaofeng.,Dong, Yue.,Duan, Tianjiao.,Zhang, Jing.,...&Dong, Yuming.(2020).A Mixed Micellar Liquid Chromatography with Direct Injection for Rapid Analysis of Eight Sulfonamides in Milk.Food Analytical Methods,13(5),1148-1158. |
MLA | Duan, Xiaoyun,et al."A Mixed Micellar Liquid Chromatography with Direct Injection for Rapid Analysis of Eight Sulfonamides in Milk".Food Analytical Methods 13.5(2020):1148-1158. |
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