Quantitative analysis method for FTIR and exploration on rheological parameters of aging asphalt binders
Li, Ping1,2; Nian, Tengfei1; Wei, Dingbang3; Lin, Mei1,2
2018-02-23
发表期刊Huazhong Keji Daxue Xuebao (Ziran Kexue Ban)/Journal of Huazhong University of Science and Technology (Natural Science Edition)
ISSN16714512
卷号46期号:2页码:34-39
摘要In order to link the chemical analysis with the pavement performance of asphalt binders, and establish a standardized and unified quantitative analysis method for Fourier transform infrared spectroscopy (FTIR), the asphalt binders of rolling thin film oven test (RTFOT) and pressure aging vessel (PAV) before and after aging were characterized by FTIR through macroscopic and microscopic methods. FTIR spectral quantitative analysis of functional change index and the complex shear modulus and phase angle of asphalt binders in dynamic shear rheometer (DSR) test under different temperature and controlled stress were conducted multivariate statistical regression analysis based on Levenberg-Macquarie method and general universal optimization algorithm. The results show that the absorption peak area of FTIR spectrum is calculated with the tangent line of the lowest point on both sides of the absorption peak, and the standard of FTIR quantitative analysis is with 2 000~650 cm-1 as the reference spectral range. The absorption peaks of 1 700 cm-1 carbonyl and 1 031 cm-1 sulfoxide increase with the increase of aging time. The complex shear modulus and phase angle of the asphalt binder after RTFOT and PAV show a multiple linear relationship with the change of chemical functional groups. © 2018, Editorial Board of Journal of Huazhong University of Science and Technology. All right reserved.
关键词Absorption spectroscopy Asphalt Asphalt pavements Binders Elastic moduli Fourier transform infrared spectroscopy Multivariant analysis Regression analysis Shear strain Spectrum analysis Asphalt binders Characteristic functional group index Chemical functional groups Dynamic shear rheometer Macroscopic and microscopic Rheological parameter Rolling thin-film oven tests Statistical regression analysis
DOI10.13245/j.hust.180207
收录类别EI
语种中文
出版者Huazhong University of Science and Technology
EI入藏号20181004876931
EI主题词Chemical analysis
来源库Compendex
分类代码411.1 Asphalt - 801 Chemistry - 803 Chemical Agents and Basic Industrial Chemicals - 922 Statistical Methods - 922.2 Mathematical Statistics - 931.1 Mechanics - 951 Materials Science
引用统计
文献类型期刊论文
条目标识符https://ir.lut.edu.cn/handle/2XXMBERH/114109
专题土木工程学院
作者单位1.School of Civil Engineering, Lanzhou University of Technology, Lanzhou; 730050, China;
2.Western Engineering Research Center of Disaster Mitigation in Civil Engineering of Ministry of Education, Lanzhou University of Technology, Lanzhou; 730050, China;
3.Gansu Changlong Highway Maintenance Technology Institute Co. Ltd., Lanzhou; 730000, China
第一作者单位土木工程学院
第一作者的第一单位土木工程学院
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GB/T 7714
Li, Ping,Nian, Tengfei,Wei, Dingbang,et al. Quantitative analysis method for FTIR and exploration on rheological parameters of aging asphalt binders[J]. Huazhong Keji Daxue Xuebao (Ziran Kexue Ban)/Journal of Huazhong University of Science and Technology (Natural Science Edition),2018,46(2):34-39.
APA Li, Ping,Nian, Tengfei,Wei, Dingbang,&Lin, Mei.(2018).Quantitative analysis method for FTIR and exploration on rheological parameters of aging asphalt binders.Huazhong Keji Daxue Xuebao (Ziran Kexue Ban)/Journal of Huazhong University of Science and Technology (Natural Science Edition),46(2),34-39.
MLA Li, Ping,et al."Quantitative analysis method for FTIR and exploration on rheological parameters of aging asphalt binders".Huazhong Keji Daxue Xuebao (Ziran Kexue Ban)/Journal of Huazhong University of Science and Technology (Natural Science Edition) 46.2(2018):34-39.
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