Effects of sintering temperature on mechanical properties and microstructure of 20% ZrO2(3Y)/Al2O3 composite ceramics
Wang, Bing-Jun1; Wang, Xiao-Min1,2; La, Pei-Qing2
2015-10-20
发表期刊Cailiao Gongcheng/Journal of Materials Engineering
ISSN10014381
卷号43期号:10页码:66-72
摘要20% nano ZrO2 (3Y) powders were added to high purity submicron Al2O3 powders, then composite ceramics were prepared by high-pressure dry pressing and constant heating, multi-stage, short insulation sintering method at different temperatures. The effect of sintering temperature on mechanical properties of composite ceramics was investigated, the phase composition and microstructure of composite ceramics were analyzed by XRD, EDS and SEM. The results show that the sintering temperature affects the mechanical properties and microstructure of composite ceramics greatly. The relative density, vickers hardness and fracture toughness reach the maximum value, respectively 98.6%, 18.54 GPa and 9.3 MPa·m1/2 under atmospheric sintering at 1600 and insulation 8h. While the grain size of the matrix is about 1.4-8.1 μm and ZrO2 phase transition is 34.6%. Composite ceramics have excellent microstructure sintered at 1600. The fracture mode of the composite ceramics is intergranular-transgranular mixed fracture mode. The fracture toughness of the composite ceramics is improved by phase transition toughening, intragranular particles toughening, crack deflection and other aspects when adding nano-sized ZrO2 (3Y) powder. ©, 2015, Beijing Institute of Aeronautical Materials (BIAM). All right reserved.
关键词Alumina Aluminum oxide Ceramic materials Fracture toughness Mechanical properties Microstructure Powders Sintering Textures Vickers hardness Zirconia Atmospheric sintering Composite ceramic Crack deflections Intragranular particles Phase transition toughening Properties and microstructures Properties of composites Sintering temperatures
DOI10.11868/j.issn.1001-4381.2015.10.011
收录类别EI
语种中文
出版者Beijing Institute of Aeronautical Materials (BIAM)
EI入藏号20154701563266
EI主题词Yttrium compounds
EI分类号804.2 Inorganic Compounds - 951 Materials Science
来源库Compendex
分类代码804.2 Inorganic Compounds - 812.1 Ceramics - 951 Materials Science
引用统计
文献类型期刊论文
条目标识符https://ir.lut.edu.cn/handle/2XXMBERH/112854
专题材料科学与工程学院
作者单位1.School of Mechanical Engineering, Qinghai University, Xining; 810016, China;
2.State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metals, Lanzhou University of Technology, Lanzhou; 730050, China
推荐引用方式
GB/T 7714
Wang, Bing-Jun,Wang, Xiao-Min,La, Pei-Qing. Effects of sintering temperature on mechanical properties and microstructure of 20% ZrO2(3Y)/Al2O3 composite ceramics[J]. Cailiao Gongcheng/Journal of Materials Engineering,2015,43(10):66-72.
APA Wang, Bing-Jun,Wang, Xiao-Min,&La, Pei-Qing.(2015).Effects of sintering temperature on mechanical properties and microstructure of 20% ZrO2(3Y)/Al2O3 composite ceramics.Cailiao Gongcheng/Journal of Materials Engineering,43(10),66-72.
MLA Wang, Bing-Jun,et al."Effects of sintering temperature on mechanical properties and microstructure of 20% ZrO2(3Y)/Al2O3 composite ceramics".Cailiao Gongcheng/Journal of Materials Engineering 43.10(2015):66-72.
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