Study on preparation of nanosized Sb and dispersion of Sb in liquid media

doi:10.3969/j.issn.1005-5053.2012.1.012

	Study on preparation of nanosized Sb and dispersion of Sb in liquid media
	Xu, Jian-Lin1,2 ; Yang, Shu-Hua 1,2; Gao, Wei 3; Kang, Zhao 1,2; Gu, Yu-Fen1,2 ; Zhang, Jian-Bin1,2
	2012-02-01
发表期刊	Hangkong Cailiao Xuebao/Journal of Aeronautical Materials
ISSN	10055053
卷号	32 期号:1 页码:57-62
摘要	Nano antimony particles with different morphology and size were prepared by electrochemical method (Electrodeposition), while the surface was modified by using OP-10. Some methods such as TEM, XRD, FTIR were used for the morphology, size and coating effects analysis of the nanometer-sized Sb particles. The results showed that there were time effects and current effects when antimony nanoparticles were synthesized. With increasing reaction time, the size of nano-antimony particle became larger and, to some extent, agglomerating phenomenon of nano-antimony particle occurred. When the current density changed within a certain range, the suitable increase of the current density was conducive to the formation of nano-antimony particles. The surface modification of nano-particles of antimony was obtained mainly by coating of OP-10 through chemical absorption between OP-10 long-chain molecular structure and nano-antimony particle, interaction of hydrogen bond and van der waals force among OP-10 long-chain alkyl molecular, mutual tangle of molecular chain and mutual permeation of C-H bond, while the bond of ether playing a role during the reaction. The dispersion and stability of nano antimony particles in the pure liquid paraffin oil related to their dosage, and the optimum amount is 0.5%.
关键词	Chemical modification Coatings Dispersion (waves) Dispersions Hydrogen bonds Morphology Nanoparticles Paraffin oils Particle size analysis Synthesis (chemical) Van der Waals forces Chemical absorption Current effect Effects analysis ELectrochemical methods Molecular chains Morphology and size Nanometer sb particles Preparation
DOI	10.3969/j.issn.1005-5053.2012.1.012
收录类别	EI
语种	中文
出版者	Chinese Journal of Aeronautics
EI入藏号	20121214874171
EI主题词	Antimony
EI分类号	513.3 Petroleum Products - 546.4 Antimony and Alloys - 761 Nanotechnology - 801.4 Physical Chemistry - 802.2 Chemical Reactions - 813.2 Coating Materials - 933 Solid State Physics - 951 Materials Science
来源库	Compendex
分类代码	513.3 Petroleum Products - 546.4 Antimony and Alloys - 761 Nanotechnology - 801.4 Physical Chemistry - 802.2 Chemical Reactions - 813.2 Coating Materials - 933 Solid State Physics - 951 Materials Science
引用统计	无
文献类型	期刊论文
条目标识符	https://ir.lut.edu.cn/handle/2XXMBERH/111387
专题	材料科学与工程学院省部共建有色金属先进加工与再利用国家重点实验室
作者单位	1.State Key Laboratory of Gansu Advanced Non-Ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China; 2.Key Laboratory of Non-Ferrous Metal Alloys and Processing, The Ministry of Education, Lanzhou University of Technology, Lanzhou 730050, China; 3.Product Development Department, Beijing Institute of Aeronautical Material, Beijing 100095, China
第一作者单位	省部共建有色金属先进加工与再利用国家重点实验室; 兰州理工大学
第一作者的第一单位	省部共建有色金属先进加工与再利用国家重点实验室
推荐引用方式 GB/T 7714	Xu, Jian-Lin,Yang, Shu-Hua,Gao, Wei,et al. Study on preparation of nanosized Sb and dispersion of Sb in liquid media[J]. Hangkong Cailiao Xuebao/Journal of Aeronautical Materials,2012,32(1):57-62.
APA	Xu, Jian-Lin,Yang, Shu-Hua,Gao, Wei,Kang, Zhao,Gu, Yu-Fen,&Zhang, Jian-Bin.(2012).Study on preparation of nanosized Sb and dispersion of Sb in liquid media.Hangkong Cailiao Xuebao/Journal of Aeronautical Materials,32(1),57-62.
MLA	Xu, Jian-Lin,et al."Study on preparation of nanosized Sb and dispersion of Sb in liquid media".Hangkong Cailiao Xuebao/Journal of Aeronautical Materials 32.1(2012):57-62.