Synthesis of zeolite 4A from kaolin and its adsorption equilibrium of carbon dioxide

doi:10.3390/ma12091536

	Synthesis of zeolite 4A from kaolin and its adsorption equilibrium of carbon dioxide
	Wang, Peng 1; Sun, Qi 1; Zhang, Yujiao 2; Cao, Jun 1
	2019
发表期刊	Materials
ISSN	1996-1944
卷号	12 期号:9
摘要	Zeolite 4A was successfully prepared by hydrothermal synthesis using low-grade kaolin as a raw material. The properties of the synthesized zeolite 4A were characterized by means of X-ray diffraction (XRD), Fourier transform infrared (FTIR), 29Si magic-angle spinning (MAS)-nuclear magnetic resonance (NMR) and 27Al MAS-NMR, X-ray fluorescence (XRF), scanning electron microscopy (SEM)-energy-dispersive spectrometry (EDS), transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET), thermogravimetry (TG)-differential thermal analysis (DTA), and carbon dioxide adsorption analysis. The textural properties of the synthesized zeolite 4A was further studied by BET analysis technique. The thermal stability analysis showed that the heat resistance of the synthesized zeolite 4A is up to 940 °C. In addition, it is found that the Langmuir model has the best agreement with the adsorption equilibrium data for carbon dioxide by synthesized zeolite 4A and commercial zeolite 4A. Meanwhile, the carbon dioxide adsorption analysis confirmed that the maximum equilibrium adsorption amount of carbon dioxide on synthesized zeolite 4A is 59.3820 mL/g, which is higher than the 55.4303 mL/g of the commercial zeolite 4A. © 2019 by the authors.
关键词	Adsorption isotherms Carbon dioxide Differential thermal analysis Fourier transform infrared spectroscopy Heat resistance High resolution transmission electron microscopy Hydrothermal synthesis Kaolin Magic angle spinning Scanning electron microscopy Thermogravimetric analysis Zeolites Adsorption equilibria Brunauer emmett tellers Carbon dioxide adsorption Differential thermal analyses (DTA) Energy dispersive spectrometry Fourier transform infrared Nuclear magnetic resonance(NMR) Zeolite 4A
DOI	10.3390/ma12091536
收录类别	EI ; SCIE
语种	英语
资助项目	Introducing talent project [Guizhou University, Guiyang (2015)][13]
WOS研究方向	Materials Science
WOS类目	Materials Science, Multidisciplinary
WOS记录号	WOS:000469757500177
出版者	MDPI AG, Postfach, Basel, CH-4005, Switzerland
EI入藏号	20192106947372
EI主题词	Gas adsorption
来源库	Compendex
分类代码	482.2 Minerals - 741.3 Optical Devices and Systems - 801 Chemistry - 802.2 Chemical Reactions - 802.3 Chemical Operations - 804.2 Inorganic Compounds - 931.2 Physical Properties of Gases, Liquids and Solids
引用统计	被引频次：28[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	https://ir.lut.edu.cn/handle/2XXMBERH/114212
专题	兰州理工大学省部共建有色金属先进加工与再利用国家重点实验室
通讯作者	Sun, Qi
作者单位	1.Guizhou Univ, Coll Mat & Met, Guiyang 550025, Guizhou, Peoples R China; 2.Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China
推荐引用方式 GB/T 7714	Wang, Peng,Sun, Qi,Zhang, Yujiao,et al. Synthesis of zeolite 4A from kaolin and its adsorption equilibrium of carbon dioxide[J]. Materials,2019,12(9).
APA	Wang, Peng,Sun, Qi,Zhang, Yujiao,&Cao, Jun.(2019).Synthesis of zeolite 4A from kaolin and its adsorption equilibrium of carbon dioxide.Materials,12(9).
MLA	Wang, Peng,et al."Synthesis of zeolite 4A from kaolin and its adsorption equilibrium of carbon dioxide".Materials 12.9(2019).