One-step hydrothermal synthesis of zeolite KA from kaolin

doi:10.1049/mnl.2019.0190

	One-step hydrothermal synthesis of zeolite KA from kaolin
	Wang, Peng 1; Sun, Qi 1; Zhang, Yujiao 2; Cao, Jun 1
	2019
发表期刊	Micro and Nano Letters
卷号	14 期号:13 页码:1298-1302
摘要	This work reports an experimental investigation on the synthesis of zeolite KA by one-step hydrothermal method using kaolin as the main SiO2 and Al2O3 sources. The phase, structure, microscopic morphology, microstructure, specific surface area, and thermal stability of the produced zeolite KA were characterised in detail. The zeolite KA was successfully synthesised and the characterisation of the obtained material was carried out considering different techniques, including X-ray diffraction, Fourier transform infrared, scanning electron microscopy, transmission electron microscopy (TEM), Brunauer–Emmett–Teller (BET) and thermogravimetric differential thermal analyser (TG-DSC). TEM analysis indicated the formation of body-centred cubic crystal zeolite KA and the polycrystallinity of the zeolite KA structure. The BET study confirmed that a total surface area of 13.2771 m2 g−1, micropore surface area of 1.3598 m2 g−1 and micropore volume of 0.000556 cm3 g−1 are obtained. In addition, the thermal stability of the zeolite KA was further studied by TG-DSC. © The Institution of Engineering and Technology 2019
关键词	Alumina Aluminum oxide Crystal structure High resolution transmission electron microscopy Kaolin Microporosity Morphology Scanning electron microscopy Silica Thermoanalysis Thermodynamic stability Zeolites Body-centred cubic Differential thermals Experimental investigations Fourier transform infra reds Hydrothermal methods Microscopic morphology Thermo-gravimetric Total surface area
DOI	10.1049/mnl.2019.0190
收录类别	EI ; SCIE
语种	英语
WOS研究方向	Science & Technology - Other Topics ; Materials Science
WOS类目	Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary
WOS记录号	WOS:000503179600003
出版者	Institution of Engineering and Technology
EI入藏号	20194607684069
EI主题词	Hydrothermal synthesis
EI分类号	482.2 Minerals - 641.1 Thermodynamics - 741.3 Optical Devices and Systems - 801 Chemistry - 802.2 Chemical Reactions - 804.2 Inorganic Compounds - 931.2 Physical Properties of Gases, Liquids and Solids - 933.1.1 Crystal Lattice
来源库	Compendex
分类代码	482.2 Minerals - 641.1 Thermodynamics - 741.3 Optical Devices and Systems - 801 Chemistry - 802.2 Chemical Reactions - 804.2 Inorganic Compounds - 931.2 Physical Properties of Gases, Liquids and Solids - 933.1.1 Crystal Lattice
引用统计	被引频次：2[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	https://ir.lut.edu.cn/handle/2XXMBERH/113985
专题	兰州理工大学
通讯作者	Sun, Qi
作者单位	1.Guizhou Univ, Coll Mat & Met, Guiyang 550025, Guizhou, Peoples R China; 2.Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China
推荐引用方式 GB/T 7714	Wang, Peng,Sun, Qi,Zhang, Yujiao,et al. One-step hydrothermal synthesis of zeolite KA from kaolin[J]. Micro and Nano Letters,2019,14(13):1298-1302.
APA	Wang, Peng,Sun, Qi,Zhang, Yujiao,&Cao, Jun.(2019).One-step hydrothermal synthesis of zeolite KA from kaolin.Micro and Nano Letters,14(13),1298-1302.
MLA	Wang, Peng,et al."One-step hydrothermal synthesis of zeolite KA from kaolin".Micro and Nano Letters 14.13(2019):1298-1302.